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Reduction Tube

Posted: 08 Mar 2023, 14:36
by Graham Kemp
Has anyone made a Reduction Tube for the reduction of Copper(II) oxide with Methane gas?

Apparently, it requires heating a stoppered boiling tube over a bunsen flame until the expanding air bursts a hole through the side!

:w00t: I've done some glasswork before, but I'm nervous to try this.

Better yet, may I buy one premade from a supplier. I can't seem to find a catalogue listing for "Reduction Tube", but perhaps there's another name to search?

Re: Reduction Tube

Posted: 14 Mar 2023, 10:33
by mtg
I have a stack of copper reduction tubes, never used in my life time, they are a glass tube, roughly 11mm in diameter, with a bubble (sort of) in the middle, about 30mm wide, 180mm long all up.

Re: Reduction Tube

Posted: 16 Mar 2023, 09:10
by bigmack
mtg wrote: 14 Mar 2023, 10:33 I have a stack of copper reduction tubes, never used in my life time, they are a glass tube, roughly 11mm in diameter, with a bubble (sort of) in the middle, about 30mm wide, 180mm long all up.
Any chance of a pic mtg ?

Re: Reduction Tube

Posted: 16 Mar 2023, 10:27
by Marama T